AX-2026-042160
GHRP-2 · 5 mg declared · Hunan Aslsen Technology Co., Ltd. · lot HOMO-2602-E9033
- Report ID
- AX-2026-042160
- Compound
- GHRP-2
- Compound class
- Growth-hormone axis peptides
- Supplier
- Homopeptide — Hunan Aslsen Technology Co., Ltd.
- Batch / lot
- HOMO-2602-E9033
- Declared label claim
- 5mg
- Laboratory
- Medutest
- Assay date
- 26 May 2026
- Submitted
- 11 Jun 2026
- Quarter
- 2026-Q2
- Submitter
- o.novak
- Sample provenance
- Supplier-supplied
Results
Measured against the index acceptance specification for the growth-hormone axis peptides class. A specification is a decision the index made; a result is a measurement. See where each threshold came from.
| Parameter | Method | Result | Unit | Index spec | |
|---|---|---|---|---|---|
| Purity | RP-HPLC, 25 min gradient, 214 nm | 99.62 | % area | ≥ 99.0 | PASS |
| Total impurities | RP-HPLC, sum of reported peaks | 0.38 | % area | ≤ 1.0 | PASS |
| Largest single impurity | RP-HPLC — C-terminal free acid (+1 Da) | 0.19 | % area | ≤ 1.00 | PASS |
| Identity — theoretical monoisotopic mass | calculated from molecular formula | 817.4275 | Da | — | NOT TESTED |
| Identity — observed monoisotopic mass | LC-MS, unit resolution (single quadrupole) | 817.4273 | Da | — | NOT TESTED |
| Mass accuracy | observed vs theoretical | -0.2 | ppm | ± 15 | PASS |
| Total peptide content | by difference from the gravimetric mass balance | 89.63 | %w/w | — | NOT TESTED |
| Target-compound content | total peptide content × purity | 89.29 | %w/w | — | NOT TESTED |
| Gross fill (as weighed) | five-place balance, under nitrogen | 5.57 | mg | 5 mg declared | NOT TESTED |
| Recovered target peptide | gross fill × target content | 4.973 | mg | 5 mg claim | NOT TESTED |
| Recovery against label claim | recovered ÷ claim | 99.5 | % | 90.0 – 110.0 | PASS |
| Water content | Karl Fischer, coulometric, duplicate | 4.50 | % | ≤ 9.0 | PASS |
| Counter-ion (acetate) | anion-exchange ion chromatography | 5.27 | % | ≤ 12.0 | PASS |
| Residual solvent + inorganic residue | estimated — see /methods/residual-solvents-q3c/ | 0.60 | % | — | NOT TESTED |
| Endotoxin | not ordered on this submission | not determined | — | ≤ 5.0 | NOT TESTED |
| Sterility | not ordered on this submission | not determined | — | no growth | NOT TESTED |
| Appearance | visual, diffuse light, black and white background | White lyophilised cake, intact | — | white to off-white intact cake | PASS |
| Reconstitution clarity | reconstituted per submitter procedure | Clear with a single visible fibre | — | clear, no visible particulates | FAIL |
| pH (reconstituted, 1 mg/mL) | potentiometric, two-point calibration | 5.56 | — | 2.5 – 8.0 | PASS |
| Retention time (observed) | RP-HPLC, 25 min gradient | 7.81 | min | 7.67 ± 0.25 (normalised) | PASS |
| Peak asymmetry (10 % height) | Ph. Eur. 2.2.46 | 1.13 | — | 0.80 – 1.50 | PASS |
| Plate count, main peak | N = 5.54 (t/w½)² | 63,995 | — | ≥ 20,000 | PASS |
| Resolution to nearest impurity | vs [D-2-Nal]-epimer | 0.92 | — | no index criterion | REPORTED |
Chromatogram and peak integration
The figure is drawn from the table. It is not an independent illustration — if a number in the table changed, the trace would change with it.
| # | Peak | RT | Area (µV·s) | % area | Δ mass (Da) |
|---|---|---|---|---|---|
| 1 | GHRP-2 — main peak | 7.81 | 4,841,841 | 99.62 | — |
| 2 | C-terminal free acid (+1 Da) | 7.94 | 9,235 | 0.19 | +0.984 |
| 3 | oxidised Trp (+16 Da) | 7.51 | 4,860 | 0.10 | +15.995 |
| 4 | des-Lys (−128 Da) | 7.61 | 2,430 | 0.05 | -128.095 |
| 5 | [D-2-Nal]-epimer | 7.69 | 1,944 | 0.04 | 0.000 |
| Closure check — purity + Σ impurities | 100.00 | CLOSES | |||
Reporting threshold 0.05 % area. Peaks below it are not reported and are therefore excluded from the total, which overstates purity by their sum — see peak integration.
Mass spectrum and identity
Theoretical monoisotopic mass 817.4275 Da, computed from C45H55N9O6. All ppm figures on this site are against monoisotopic values — see why that matters.
| Charge | Theoretical m/z | Observed m/z | Δ m/z | Rel. abundance (%) |
|---|---|---|---|---|
| 2+ | 409.7210 | 409.7209 | -0.0001 | 52.0 |
| 1+ | 818.4348 | 818.4346 | -0.0002 | 100.0 |
Gravimetric mass balance
Water, counter-ion, residual and total peptide content are exhaustive and mutually exclusive categories. They must account for 100 % of the cake mass. The index closes this to within 0.02 pp and the build asserts it.
| Component | Determination | %w/w of cake |
|---|---|---|
| Water | Karl Fischer | 4.50 |
| Counter-ion (acetate) | ion chromatography | 5.27 |
| Residual solvent + inorganic residue | estimated | 0.60 |
| Total peptide content | by difference | 89.63 |
| Total | 100.00 CLOSES | |
Supplier certificate, as declared
The supplier's own figures for this lot, beside the independent measurement. Divergence is assessed against the batch median, not against this single report — see rule AX-R05.
| Figure | Supplier COA | This report | Index note |
|---|---|---|---|
| Purity (% area) | 99.90 | 99.62 | divergence +0.28 pp vs batch median |
| Total impurities (% area) | 0.10 | 0.38 | |
| Largest single impurity (% area) | 0.05 | 0.19 | |
| Water (%) | 2.2 | 4.50 | |
| Counter-ion (%) | not stated | 5.27 | |
| Peptide content (%w/w) | not stated | 89.63 | |
| Endotoxin (EU/mg) | not stated | not determined | |
| Method stated on certificate | YES | — | column, gradient and wavelength given |
Provenance and caveats
Where a sample came from changes the weight of the evidence. The index treats it as a first-class field.
- Sample provenance
- Supplier-supplied
- Evidentiary weight
- Weaker evidence. Read with the caveat below.
- Chain of custody
- Supplier despatch → laboratory direct (courier, cold pack, 11 d) → assay. Submitter did not handle the vial.
- Assay date
- 26 May 2026
- Submitted to the index
- 11 Jun 2026
- Laboratory
- Medutest, Ljubljana, Slovenia
- Method basis
- 25 min gradient · unit-resolution MS
- Verification status
- IDENTITY CONSISTENT
Annotations
No annotations on this record. Annotations are short signed technical comments from index contributors; see how to contribute.
Related records
Same batch — lot HOMO-2602-E9033 n=5
| Report | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|
| AX-2026-042157 | HOMO-2602-E9033 | PeptideMeter | 2026-Q2 | 99.93 | 4.32 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042158 | HOMO-2602-E9033 | Janoshik | 2026-Q2 | 99.59 | 4.35 | 89.8 | Buyer-sourced | 2 | MARGINAL |
| AX-2026-042159 | HOMO-2602-E9033 | Janoshik | 2026-Q2 | 99.39 | 3.77 | — | Laboratory-retained | 1 | MARGINAL |
| AX-2026-042161 | HOMO-2602-E9033 | Medutest | 2026-Q2 | 99.93 | 3.99 | 105.6 | Supplier-supplied | 1 | MARGINAL |
Cross-sections
| Report | Supplier | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|---|
| AX-2026-042161 | Homopeptide | HOMO-2602-E9033 | Medutest | 2026-Q2 | 99.93 | 3.99 | 105.6 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042302 | HJ | HJ-2602-W3148 | PeptideMeter | 2026-Q2 | 99.55 | 1.32 | 104.9 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042159 | Homopeptide | HOMO-2602-E9033 | Janoshik | 2026-Q2 | 99.39 | 3.77 | — | Laboratory-retained | 1 | MARGINAL |
| AX-2026-042303 | HJ | HJ-2602-W3148 | PeptideMeter | 2026-Q2 | 99.12 | 1.24 | 98.0 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-043489 | WXT | WXT-2605-U5824 | PeptideMeter | 2026-Q2 | 98.83 | 5.76 | 96.6 | Supplier-supplied | 2 | FAIL |
| AX-2026-042157 | Homopeptide | HOMO-2602-E9033 | PeptideMeter | 2026-Q2 | 99.93 | 4.32 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042158 | Homopeptide | HOMO-2602-E9033 | Janoshik | 2026-Q2 | 99.59 | 4.35 | 89.8 | Buyer-sourced | 2 | MARGINAL |
| AX-2026-041420 | WWB | WWB-2511-K4194 | Nordanalyt | 2026-Q1 | 99.51 | 4.94 | — | Supplier-supplied | 1 | MARGINAL |
| Report | Compound | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|---|
| AX-2026-042181 | Ipamorelin | HOMO-2608-A9045 | Janoshik | 2026-Q3 | 99.78 | 4.79 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042172 | Semaglutide | HOMO-2604-X8921 | Janoshik | 2026-Q3 | 99.64 | 5.16 | 91.9 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042278 | SLU-PP-332 | HOMO-2602-Y2822 | Kestrel | 2026-Q3 | 99.71 | 4.42 | — | Supplier-supplied | 0 | PASS |
| AX-2026-042180 | Ipamorelin | HOMO-2608-A9045 | Janoshik | 2026-Q3 | 99.39 | 4.74 | 105.5 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042184 | Ipamorelin | HOMO-2608-A9045 | Kestrel | 2026-Q3 | 99.27 | 4.79 | 103.2 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042274 | SLU-PP-332 | HOMO-2602-Y2822 | VendorInvestigate | 2026-Q3 | 98.71 | 4.72 | — | Laboratory-retained | 0 | PASS |
| AX-2026-042183 | Ipamorelin | HOMO-2608-A9045 | VendorInvestigate | 2026-Q3 | 99.38 | 4.97 | — | Buyer-sourced | 1 | MARGINAL |
| AX-2026-042194 | Retatrutide | HOMO-2605-V9833 | PeptideMeter | 2026-Q3 | 98.90 | 4.07 | 98.8 | Supplier-supplied | 3 | MARGINAL |