AssayIndex

SWB-2507-E7084

5-Amino-1MQ · 50 mg declared · Shanghai Wibson Biotechnology Co., Ltd. · manufactured 24 Jul 2025

CHARACTERISED
Lot code
SWB-2507-E7084
Supplier
SWB — Shanghai Wibson Biotechnology Co., Ltd.
Compound
5-Amino-1MQ
Compound class
Non-peptide adjuncts
Declared label claim
50mg
Manufacture date
24 Jul 2025
Index quarter
2025-Q3
Independent assays
14
Laboratories involved
Medutest, VendorInvestigate, Janoshik
Provenance mix
Buyer-sourced ×13 · Laboratory-retained ×1
Section 1

Reproducibility across independent tests

Every report below is an observation of the same physical material. What they disagree about is measurement; what they agree about is the lot. The size of the disagreement is compared against what the contributing laboratories' own repeatability figures predict.

Independent assays 14
Median purity 99.35% n=14
Spread (max − min) 1.20pp n=14
Standard deviation 0.303pp n=14
97.998.398.699.099.499.7100.1This lot (SWB-2507-E7084)This lot (SWB-2507-E7084): Q1 99.15, median 99.34, Q3 99.48, n=14n=14All 5-Amino-1MQAll 5-Amino-1MQ: Q1 99.22, median 99.47, Q3 99.66, n=94outlier 98.07outlier 98.34outlier 98.37outlier 98.41outlier 98.44outlier 98.52n=94 Purity (% area)
Figure 1. This lot's independent purity results against the whole 5-Amino-1MQ record set in the index. The vertical line is the index acceptance specification for the non-peptide adjuncts class, 98.0 % area. A narrow box on the top row against a wide box on the bottom row is the ideal reading: it means the disagreement between lots is much larger than the disagreement within this one.
Section 2

Member reports 14

Every report the index holds on this lot. Each is a page carrying its own chromatogram, mass spectrum, mass balance, provenance and caveats.

ReportLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2025-019989SWB-2507-E7084Medutest2025-Q399.476.35Buyer-sourced0FAIL
AX-2025-019990SWB-2507-E7084VendorInvestigate2025-Q399.046.00104.2Buyer-sourced0FAIL
AX-2025-019991SWB-2507-E7084VendorInvestigate2025-Q399.126.47Buyer-sourced0FAIL
AX-2025-019992SWB-2507-E7084VendorInvestigate2025-Q399.285.70Buyer-sourced0FAIL
AX-2025-019993SWB-2507-E7084VendorInvestigate2025-Q398.735.27Buyer-sourced0FAIL
AX-2025-019994SWB-2507-E7084Janoshik2025-Q399.416.32Laboratory-retained0FAIL
AX-2025-019995SWB-2507-E7084Janoshik2025-Q399.555.98Buyer-sourced0FAIL
AX-2025-019996SWB-2507-E7084VendorInvestigate2025-Q399.425.9097.5Buyer-sourced0FAIL
AX-2025-019997SWB-2507-E7084Janoshik2025-Q398.936.5489.1Buyer-sourced1FAIL
AX-2025-019998SWB-2507-E7084Janoshik2025-Q399.585.9893.4Buyer-sourced0FAIL
AX-2025-019999SWB-2507-E7084Janoshik2025-Q399.496.33101.1Buyer-sourced0FAIL
AX-2025-020000SWB-2507-E7084Janoshik2025-Q399.245.8593.3Buyer-sourced0FAIL
AX-2025-020001SWB-2507-E7084Janoshik2025-Q399.256.24Buyer-sourced0FAIL
AX-2025-020002SWB-2507-E7084VendorInvestigate2025-Q399.936.09Buyer-sourced0FAIL
Section 3

By laboratory

Where more than one laboratory assayed this lot, the difference between them is a paired observation of their relative bias — the same material, the same time window, different instruments. Those pairs are what the index's bias estimates are built from.

LaboratoryReportsPurity results (% area)MedianGradientPublished bias (pp)Bias-adjusted
Medutest199.4799.4725min+0.0899.39
VendorInvestigate699.04, 99.12, 99.28, 98.73, 99.42, 99.9399.2032min-0.1199.31
Janoshik799.41, 99.55, 98.93, 99.58, 99.49, 99.24, 99.2599.4130min+0.0099.41

This lot contributes 3 paired comparisons to the inter-lab analysis.

Section 4

The supplier's certificate for this lot

One number the supplier wrote, beside the median of the numbers other people measured on the same physical material. That comparison is only available because the index groups by lot.

FigureSupplier COAThis reportIndex note
Purity (% area)99.0899.47divergence -0.27 pp vs batch median
Total impurities (% area)not stated0.53
Largest single impurity (% area)not stated0.27
Water (%)not stated6.35
Counter-ion (%)not stated39.93
Peptide content (%w/w)91.7not determined
Endotoxin (EU/mg)0.21not determined
Method stated on certificateNOno method section — the result cannot be reconciled against any other
Section 5

Impurity fingerprint

The named impurities reported across this lot's assays, with how consistently each was seen. A fingerprint is what allows two lot numbers held by different companies to be identified as one bulk.

Named impurityReported inMedian % areaRange
free iodide (counter-ion, by IC)14 / 140.180.04–0.41
8-amino regioisomer14 / 140.130.03–0.34
1-methylquinolinium (des-amino, −15 Da)13 / 140.230.09–0.66
5-nitro-1MQ (unreduced precursor, +30 Da)13 / 140.060.02–0.15
Section 7

What this rollup does not establish