AX-2025-019618
GHRP-6 · 2 mg declared · Hunan Aslsen Technology Co., Ltd. · lot HOMO-2505-A1799
- Report ID
- AX-2025-019618
- Compound
- GHRP-6
- Compound class
- Growth-hormone axis peptides
- Supplier
- Homopeptide — Hunan Aslsen Technology Co., Ltd.
- Batch / lot
- HOMO-2505-A1799
- Declared label claim
- 2mg
- Laboratory
- Janoshik Analytical
- Assay date
- 06 Oct 2025
- Submitted
- 25 Oct 2025
- Quarter
- 2025-Q4
- Submitter
- Contributor #V-6845
- Sample provenance
- Supplier-supplied
Results
Measured against the index acceptance specification for the growth-hormone axis peptides class. A specification is a decision the index made; a result is a measurement. See where each threshold came from.
| Parameter | Method | Result | Unit | Index spec | |
|---|---|---|---|---|---|
| Purity | RP-HPLC, 30 min gradient, 214 nm | 99.93 | % area | ≥ 99.0 | PASS |
| Total impurities | RP-HPLC, sum of reported peaks | 0.07 | % area | ≤ 1.0 | PASS |
| Largest single impurity | RP-HPLC — oxidised Trp (+16 Da) | 0.04 | % area | ≤ 1.00 | PASS |
| Identity | not ordered on this submission | not determined | — | required for VERIFIED status | NOT TESTED |
| Total peptide content | by difference from the gravimetric mass balance | 89.40 | %w/w | — | NOT TESTED |
| Target-compound content | total peptide content × purity | 89.34 | %w/w | — | NOT TESTED |
| Gross fill (as weighed) | five-place balance, under nitrogen | 2.27 | mg | 2 mg declared | NOT TESTED |
| Recovered target peptide | gross fill × target content | 2.028 | mg | 2 mg claim | NOT TESTED |
| Recovery against label claim | recovered ÷ claim | 101.4 | % | 90.0 – 110.0 | PASS |
| Water content | Karl Fischer, coulometric, duplicate | 3.14 | % | ≤ 9.0 | PASS |
| Counter-ion (acetate) | anion-exchange ion chromatography | 7.01 | % | ≤ 12.0 | PASS |
| Residual solvent + inorganic residue | estimated — see /methods/residual-solvents-q3c/ | 0.45 | % | — | NOT TESTED |
| Endotoxin | not ordered on this submission | not determined | — | ≤ 5.0 | NOT TESTED |
| Sterility | not ordered on this submission | not determined | — | no growth | NOT TESTED |
| Appearance | visual, diffuse light, black and white background | White cake, partially collapsed | — | white to off-white intact cake | FAIL |
| Reconstitution clarity | reconstituted per submitter procedure | Clear, colourless, no visible particulates | — | clear, no visible particulates | PASS |
| pH (reconstituted, 1 mg/mL) | potentiometric, two-point calibration | 4.74 | — | 2.5 – 8.0 | PASS |
| Retention time (observed) | RP-HPLC, 30 min gradient | 8.42 | min | 8.44 ± 0.25 (normalised) | PASS |
| Peak asymmetry (10 % height) | Ph. Eur. 2.2.46 | 1.36 | — | 0.80 – 1.50 | PASS |
| Plate count, main peak | N = 5.54 (t/w½)² | 49,011 | — | ≥ 20,000 | PASS |
| Resolution to nearest impurity | vs [D-Trp]-epimer | 0.77 | — | no index criterion | REPORTED |
Chromatogram and peak integration
The figure is drawn from the table. It is not an independent illustration — if a number in the table changed, the trace would change with it.
| # | Peak | RT | Area (µV·s) | % area | Δ mass (Da) |
|---|---|---|---|---|---|
| 1 | GHRP-6 — main peak | 8.42 | 4,856,908 | 99.93 | — |
| 2 | oxidised Trp (+16 Da) | 8.08 | 1,944 | 0.04 | +15.995 |
| 3 | [D-Trp]-epimer | 8.30 | 1,458 | 0.03 | 0.000 |
| Closure check — purity + Σ impurities | 100.00 | CLOSES | |||
Reporting threshold 0.05 % area. Peaks below it are not reported and are therefore excluded from the total, which overstates purity by their sum — see peak integration.
Gravimetric mass balance
Water, counter-ion, residual and total peptide content are exhaustive and mutually exclusive categories. They must account for 100 % of the cake mass. The index closes this to within 0.02 pp and the build asserts it.
| Component | Determination | %w/w of cake |
|---|---|---|
| Water | Karl Fischer | 3.14 |
| Counter-ion (acetate) | ion chromatography | 7.01 |
| Residual solvent + inorganic residue | estimated | 0.45 |
| Total peptide content | by difference | 89.40 |
| Total | 100.00 CLOSES | |
Supplier certificate, as declared
The supplier's own figures for this lot, beside the independent measurement. Divergence is assessed against the batch median, not against this single report — see rule AX-R05.
| Figure | Supplier COA | This report | Index note |
|---|---|---|---|
| Purity (% area) | 100.5 | 99.93 | divergence +0.57 pp vs batch median |
| Total impurities (% area) | -0.50 | 0.07 | |
| Largest single impurity (% area) | -0.21 | 0.04 | |
| Water (%) | 1.2 | 3.14 | |
| Counter-ion (%) | not stated | 7.01 | |
| Peptide content (%w/w) | not stated | 89.40 | |
| Endotoxin (EU/mg) | not stated | not determined | |
| Method stated on certificate | YES | — | column, gradient and wavelength given |
Provenance and caveats
Where a sample came from changes the weight of the evidence. The index treats it as a first-class field.
- Sample provenance
- Supplier-supplied
- Evidentiary weight
- Weaker evidence. Read with the caveat below.
- Chain of custody
- Supplier despatch → laboratory direct (courier, cold pack, 7 d) → assay. Submitter did not handle the vial.
- Assay date
- 06 Oct 2025
- Submitted to the index
- 25 Oct 2025
- Laboratory
- Janoshik Analytical, Ostrava, Czechia
- Method basis
- 30 min gradient · high-resolution MS
- Verification status
- PURITY ONLY
Annotations
No annotations on this record. Annotations are short signed technical comments from index contributors; see how to contribute.
Related records
Same batch — lot HOMO-2505-A1799 n=3
| Report | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|
| AX-2025-019617 | HOMO-2505-A1799 | Janoshik | 2025-Q4 | 99.75 | 3.64 | — | Supplier-supplied | 3 | MARGINAL |
| AX-2026-042264 | HOMO-2505-A1799 | Nordanalyt | 2025-Q4 | 99.93 | 3.36 | — | Supplier-supplied | 3 | MARGINAL |
Cross-sections
| Report | Supplier | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|---|
| AX-2026-042290 | HJ | HJ-2603-R2258 | Janoshik | 2026-Q3 | 99.71 | 3.05 | — | Supplier-supplied | 2 | MARGINAL |
| AX-2026-042287 | HJ | HJ-2603-R2258 | VendorInvestigate | 2026-Q3 | 98.79 | 2.43 | 90.9 | Buyer-sourced | 2 | FAIL |
| AX-2026-042288 | HJ | HJ-2603-R2258 | Kestrel | 2026-Q3 | 99.93 | 2.82 | 92.8 | Supplier-supplied | 2 | MARGINAL |
| AX-2026-042289 | HJ | HJ-2603-R2258 | Janoshik | 2026-Q3 | 99.53 | 2.67 | 104.7 | Supplier-supplied | 2 | MARGINAL |
| AX-2026-042291 | HJ | HJ-2603-R2258 | Janoshik | 2026-Q3 | 99.60 | 2.94 | 101.3 | Supplier-supplied | 2 | MARGINAL |
| AX-2026-043560 | BCH | BCH-2603-Y7018 | Janoshik | 2026-Q2 | 99.25 | 5.25 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-043564 | BCH | BCH-2603-Y7018 | Medutest | 2026-Q2 | 98.44 | 4.83 | — | Buyer-sourced | 1 | FAIL |
| AX-2026-043562 | BCH | BCH-2603-Y7018 | PeptideMeter | 2026-Q2 | 98.57 | 4.52 | 97.9 | Supplier-supplied | 1 | FAIL |
| Report | Compound | Lot | Lab | Quarter | Purity % | Water % | Recovery % | Provenance | Flags | Result |
|---|---|---|---|---|---|---|---|---|---|---|
| AX-2026-042181 | Ipamorelin | HOMO-2608-A9045 | Janoshik | 2026-Q3 | 99.78 | 4.79 | — | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042172 | Semaglutide | HOMO-2604-X8921 | Janoshik | 2026-Q3 | 99.64 | 5.16 | 91.9 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042278 | SLU-PP-332 | HOMO-2602-Y2822 | Kestrel | 2026-Q3 | 99.71 | 4.42 | — | Supplier-supplied | 0 | PASS |
| AX-2026-042180 | Ipamorelin | HOMO-2608-A9045 | Janoshik | 2026-Q3 | 99.39 | 4.74 | 105.5 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042184 | Ipamorelin | HOMO-2608-A9045 | Kestrel | 2026-Q3 | 99.27 | 4.79 | 103.2 | Supplier-supplied | 1 | MARGINAL |
| AX-2026-042274 | SLU-PP-332 | HOMO-2602-Y2822 | VendorInvestigate | 2026-Q3 | 98.71 | 4.72 | — | Laboratory-retained | 0 | PASS |
| AX-2026-042183 | Ipamorelin | HOMO-2608-A9045 | VendorInvestigate | 2026-Q3 | 99.38 | 4.97 | — | Buyer-sourced | 1 | MARGINAL |
| AX-2026-042194 | Retatrutide | HOMO-2605-V9833 | PeptideMeter | 2026-Q3 | 98.90 | 4.07 | 98.8 | Supplier-supplied | 3 | MARGINAL |